Ultra-preparative: puriFlash® 5.400-UV
Ultra-preparative: puriFlash® 5.400-UV
Non-contractual picture.
System delivered without pump door.
puriFlash® 5.400-UV
Optimized for your ultra-preparative purifications
Flow rate
125mL/min
400 bar
Components
- Control unit
- Pump
- UV detector
- Fraction collector
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Solvent tray with drainage system
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2 integrated column holders
Pump
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Flow rate range: 1mL/min to 125mL/min
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Max. operational flow rate: 125mL/min
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Optimum flow rate for columns up to 60mm ID
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Flow rate accuracy: +/- 2.5 % from 3.5mL/min to 100mL/min & 5 to 320 bar
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Flow rate repeatability: < 0.25
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Flow rate linearity: 0.98 < linearity < 1
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Pressure range: 0 to 400 bar
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Max. operational pressure: 400 bar
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Quaternary gradient valve
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Gradient tolerance step: < 3.5 %
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Washing discs
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Washing pump allows circulation of water to prevent crystalline deposits on the pump piston (included in Pack-PWD)
Injection
- Injection mode: liquid
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“Load & Go” technology: with automatic 10-way valve that allows the use of loops for even more efficient injection
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Stainless steel injection loops 2mL and 20µL
Detection
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UV detector 200-400nm
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UV detector 200-800nm (included in the Pack-UVextended)
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“DAD” technology
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Multi-wavelength and scan collection over a band of 200nm (or 600nm with the Pack-UVextended)
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Spectral visualization and confirmation of purity
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Flow cell pathway: 1.0mm / 15µL
Column & holder compatibility
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Normal phase (NP)
Particle sizes: 3µm, 5µm, 10µm, 15µm, 25µm, 30µm, 50µmReverse phase (RP)
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Particle sizes: 3µm, 5µm, 10µm, 15µm, 25µm, 30µm, 50µm
Format: all preparative columns up to 60mm ID are compatible
2 integrated column holders (holder n°1: col. ≥ 20mm ID – holder n°2: col. 7.8 – 10mm ID)
Fraction collector
- Capacity:
- • 3 racks
- • 132 test tubes (18 x 150mm)
Technology:
- • Automatic cleaning of the fraction collector needle (to avoid cross-contamination with the previous purification)
- • RFID: automatic detection of the racks installed in the fraction collector
Proposed racks
- Delivery includes a choice of 3 racks from the following list:
- • Rack for test tubes:
– 13 x 73mm | 13 x 100mm | 16 x 150mm
– 18 x 150mm | 18 x 180mm | 21 x 150mm
– 25 x 150mm | 28 x 150mm | 29.5 x 200mm - • Rack for 250mL Schott bottles
- • Rack for funnels (in option)
- .
Position of the numbered tubes (to facilitate identification of the tubes)
Software and control unit
- Control via InterSoft® X software included:
- • Genius, Artificial Intelligence
- • “Boost & Go”™ technology
- Windows 10
Remote control
Touchscreen 15″
8 USB ports
2 RJ45 ports
Bluetooth/Wi-Fi key
System optimization
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Tubing after pump: 0.5 & 0.75mm internal diameter
Flow cell pathway: 1.0mm / 15µL
Safety
- System light status
Solvent tray with drainage system - Level sensor for solvents and waste
Retention tray with leak detectors - • pump
- • column holder
- • UV detector
- • valve
- • fraction collector
“Fume Enclosure” technology (allows the use of the purification system without a hood)
Materials in contact with solvents
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ETFE
PTFE
316 L Stainless steel
Hastelloy
PEEK
Kalrez
Sapphire
Ruby
Kel-F
Zirconium
PPS
Nitronic 60
Borosilicate glass
Accessories box
- Tubing with fitting & ferrules:
- • Tygon tubing for solvent tray drainage
- • Level sensor tubing (x5)
- • Suction tubes (x4)
- • ETFE tubing collector to Waste
- • SS tubing injection valve port 3 to C2 inlet
- • SS tubing injection valve port 6 to waste
- • SS tubing injection valve port 9 to C1 inlet
- • PEEK tubing repartition valve port 3 to C2 outlet
- • PEEK tubing repartition valve port 4 to UV cell inlet
- • PEEK tubing repartition valve port 5 to C1 outlet
- • PEEK tubing BPR outlet to collector inlet
- • PEEK tubing UV cell outlet to BPR inlet
- • SS port for injection (injection valve port 1)
- • Loop 2mL
- • Loop 20µL
- • External UV cell 1mm PEEK
- • BPR 100PSI
- • Column holder clip 12mm
- • UV cell support
- • Union 1/16”
PWD accessories:
- • PWD Tubing Kit
Cables :
- • RFID cable (x4)
- • USB/USB cable – unit control to fraction collector
- • Power cord – screen to fraction collector
- • HDMI cable – screen to unit control
- • USB/MINI USB cable – screen to unit control
- • LED’S cable – unit control to fraction collector
- • Communication cable Sub-D9 male/female (1m) – unit control to fraction collector
- • Communication cable Sub-D9 male/female (0.5m) – unit control to pump
- • Communication cable Sub-D9 female/female (1m) – unit control to UV detector
- • Power cord – pump to fraction collector + unit control to fraction collector (x2)
- • General power cable (model according to the country of destination)
Solvent tray
Clips P
Screw CHC M4x8
Grower M4 (x3)
Stylus with its clip
UV cell test
Rear fastening (x2)
Screws BHC 4×10 (x2)
UV trapdoor - iELSD trapdoor
Racks (x3)
Compliance report
Communication
Communication cable Sub-D9 male/female (1m) – unit control to fraction collector
Communication cable Sub-D9 male/female (0.5m) – unit control to pump
Communication cable Sub-D9 female/female (1m) – unit control to UV detector
Power supply
110V or 220V
Dimensions
Weight: 50kg